刘宝圣,段永生,马育松,郭春海.顶空进样气相色谱质谱法同时检测食品包装材料中的10种残留溶剂[J].食品安全质量检测学报,2013,4(6):1853-1858
顶空进样气相色谱质谱法同时检测食品包装材料中的10种残留溶剂
Determination of 10 residual solvents in food packaging material by headspace gas chromatography-mass spectrometry
投稿时间:2013-09-17  修订日期:2013-11-16
DOI:
中文关键词:  食品包装材料  溶剂残留  顶空气相色谱质谱(HS-GC/MS)  选择离子扫描(SIM)
英文关键词:food packaging material  residual solvents  headspace-gas chromatography/mass spectrometry  selected ion monitoring
基金项目:
作者单位
刘宝圣 河北出入境检验检疫局 
段永生 河北出入境检验检疫局 
马育松 河北出入境检验检疫局 
郭春海 河北出入境检验检疫局 
AuthorInstitution
LIU Bao-Sheng Hebei Entry-Exit Inspection and Quarantine Bureau 
DUAN Yong-Sheng Hebei Entry-Exit Inspection and Quarantine Bureau 
MA Yu-Song Hebei Entry-Exit Inspection and Quarantine Bureau 
GUO Chun-Hai Hebei Entry-Exit Inspection and Quarantine Bureau 
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中文摘要:
      目的 建立顶空气相色谱-质谱检测食品包装材料中10种残留有机溶剂的分析方法。方法 采用GC-MS选择离子监测(SIM)模式进行定量分析。结果 10种溶剂在0.001~0.1 mg/m2浓度范围线性关系良好, 相关系数在0.9999~1.0000, 对最低浓度点进行了重现性实验, RSD均小于10%, 回收率79.0%~106.2%, 精密度1.08%~8.02%。结论 此方法快速、准确可以满足国内外对食品包装材料中10种残留有机溶剂的同时检测。
英文摘要:
      Objective To establish a method for the determination of 10 residual solvents released from the food packaging material by the headspace gas chromatography-mass spectrometry. Methods The method was established by gas chromatography mass spectrum with selected ion monitor (GC-MS/SIM). Results The linear range of 10 residual solvents were 0.001~0.1 mg/m2 with correlative coefficient of0.9999~1.00000. The coefficient of variation was<10% on the lowest concentration. The average recoveries were 79.0%~106.2% with the relative standard deviations (RSD) of 1.08%~8.02%. Conclusion This analysis method is rapid and accurate, and it can be used for the simultaneous determination of 10 residual solvents released from the food packaging material.
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